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    Home > Chemicals Industry > Chemical Technology > Semi-volatile organic compounds analysis technology-leaching solution preparation sulfuric acid and nitric acid method

    Semi-volatile organic compounds analysis technology-leaching solution preparation sulfuric acid and nitric acid method

    • Last Update: 2022-03-12
    • Source: Internet
    • Author: User
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    Take two samples, one for determination of moisture content, and the other for toxicity leaching experiment


    1.


    Weigh 50~100g sample in a lidded container and dry it at 105℃.


    2.


    Take an appropriate amount of a mixture of concentrated sulfuric acid and concentrated nitric acid with a mass ratio of 2:1 and add it to ultrapure water, measure the pH with a pH meter, and adjust the solution to make the pH 3.


    3.


    Weigh 150~200g sample (the diameter of the sample should be less than 9.


    Note: If the sample contains the initial liquid phase, it should be carried out first


    4.


    The leachate is filtered by a high-pressure filter, and the filter membrane is made of disposable glass fiber membrane or microporous membrane (with a pore size of 0.


     

     

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