Willing Sansan

"Extracted Source" This product is the woolly plant Welling Fairy Clematis Chinensis Osbeck, cotton clump iron lotus Clematis hexapetala Pall

"Main ingredient" Zizinolic acid Oleanolic acid, content: 30%

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" Periasic ingredients" Hederagenin

tie line lotus glycoside A, iron line lotus glycoside B, iron line liglygin C Clematichinenoside A, Clematichinenoside B, Clehinenono, Huthside B Humaticozhong b

This product is light yellow to hazel coarse powder, soluble in methanol, ethanol, water-containing positive butanol

"Identification" take this product plus methanol to make 0.5% solution for test solutionTake the standard products qizifruit acid, Ivy Glycoside Yuan, iron line lotus glycoside, Weiling fairy saplycosides plus methanol to make each contain0.5 mg / ml solution as a control solutionTake The Vihring fairy standard control medicine 1.0g plus ethanol 40 ml, ultrasonic extraction for 30 minutes, the filtrate concentrates to 2 ml, divided 1ml plus hydrochloric acid 1 ml, water 10 ml, heated hydrolysis for 1 hour, cooling, chloroform extraction 3 times, chloroform steaming dry plus methanol 1 ml dissolved, mixed with unhydrolyconcentrated 1 ml concentrate for controlTake the above three liquids each 5 sl, respectively, point in the same silicone G board, toluene-ethyl ethyl ethyl-forely acid (20:3:0.2) to expand, spray 10% sulphate ethanol solution, hot wind blowingThe corresponding location of the label spot shows the same color spot, compared to the standard medicinal spot, the corresponding rate is 60%

Check DryWeight: No more than 3.0% (Appendix IXG)

burning residue: No more than 0.3% (Appendix IXJ)

Heavy Metals: Not over 10ppm (Appendix IXE)

"Content Determination" according to the high-efficiency liquid chromatography (Appendix VID) measurement

chromatographic condition C18 bar

flow phase: acetylene water (90:10)

detection wavelength: 205nm

the number of theoretical boards is 3000

control liquid: take the zigacid standard with methanol to make a 1 mg /ml solution spare

test solution: Take this product with methanol to make a 3 mg / ml solution spare

determination: take the above-mentioned two liquid injection liquid chromatography of 10 ?l injection liquid, and calculate the total triamcinol content

anti-inflammatory, anti-spasms, swelling, analgesia, anti-tumor, increase bile secretion, lower blood pressure

"storage" cool, dry, to avoid light