Volatile oil of the oil pine section

Extractsource: This product is a volatile oil ingredient extracted from the sections of Pine vegetable oil pinus tabulae ormis Carr., Masnus massonzana Lamb., with a total volatile oil content of more than 80%main ingredients: a-Penne, content: 50%p style"text-style"text-center;" align"img alt""oil-seamount volatile oil" src"/uploads/allimg/1702/2-1F2011Q52Z1.jpg"style: "style: 101px;" height: 109px;..) beta-penene-pineneL-Camphenedielene dipentenecontent: 30%the product is light yellow to yellow brown clarified, transparent liquid, soluble in petroleum ether, ethyl, chloroform, benzenerelative density of : 0.85 to 0.87refractive index: 1.466 to 1.477"Identification" take this product plus ethyl acetate to make 0.5% solution for test ingeTake the standard product seine, terpene, dielene plus ethyl acetate to make each containing 10 sl/ml solution for controlTake oil pine standard control of 1.0g plus petroleum ether 30 ml, ultrasonic extraction for 30 minutes, filter cold wind blowing out of petroleum ether, plus ethyl acetate 1 ml dissolved as a control liquidTake the above three liquid s3 sl, respectively, point on the same silicone G board, to oil ether-acetate (17:3) to expand, spray vanilla aldehyde sulfuric acid test liquid, hot air showThe corresponding position of the standard speckle appears the same color spot, compared to the standard medicinal spot, the corresponding rate of 60%" fat oil: take this product 1g plus ethanol 10 ml, shake well placed, no oil dropoutheavy metals: no more than 10 ppm (appendix IX.E) content determination: Gas chromatography (appendix VI.E) measurement chromatography conditions Column: Elastic Quartz Capillary Column (0.32mm x 30m) fixed phase: cross-linked 5% phenyl methyl polysioxyane (DB-5) film thickness: 0.25 m program heating up: 600 degrees C (5 minutes) - 5 degrees C / minute , 160 degrees C , 70 degrees C / minute , 300 degrees C (10 minutes) inlet temperature: 200 degrees C detector temperature: 320 degrees C shunt ratio: 5:1 number of theory boards: 25000 control fluid: take alpha-ethyl standard and ethanol to make 0.2mg/ml solution backup test solution: take this product plus ethanol to make 0.4mg/ml solution backup the determination: take the above two-liquid 1 sl injection gas chromatography Volatile Oil Determination: The Volatile Oil Measurement (Appendix XD) is measured the functional theme to relieve pain For rheumatism use for external use storage is closed, cool and dry