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Ferrate(1-), [N,N′-1,3-propanediylbis[N-[(carboxy-κO)methyl]glycinato-κN,κO]]-, ammonium (1:1), (OC-6-21)- is an important chemical compound that has found widespread use in the chemical industry.
It is a synthetic route to this compound that is commonly used in the industry.
The synthesis of Ferrate(1-) involves several steps, which are outlined below:
Step 1: Preparation of the N-methyl glycine starting material
The synthesis of Ferrate(1-) begins with the preparation of the N-methyl glycine starting material.
This is accomplished by reacting glycine with methyl iodide in the presence of a base, such as sodium hydroxide.
The reaction is carried out in a solvent, such as water or a polar organic solvent, and the resulting product is extracted with a solvent, such as ether or hexane.
Step 2: Nitration of N-methyl glycine
The N-methyl glycine starting material is then nitrated using a nitrating agent, such as nitric acid or a mixture of nitric and sulfuric acids.
The reaction is typically carried out in the presence of a solvent, such as water or a polar organic solvent, and the resulting product is extracted with a solvent, such as ether or hexane.
Step 3: Condensation of N-methyl glycine with 1,3-propanediol
The nitrated N-methyl glycine is then condensed with 1,3-propanediol in the presence of a base, such as sodium hydroxide.
The reaction is carried out in a solvent, such as water or a polar organic solvent, and the resulting product is extracted with a solvent, such as ether or hexane.
Step 4: Formation of the Ferrate(1-) compound
The condensed product from step 3 is then treated with a solution of ferrous chloride in a solvent, such as water or a polar organic solvent.
The resulting product is then treated with ammonia in the presence of a solvent, such as water or a polar organic solvent.
The product is then treated with a mineral acid, such as hydrochloric acid, to form the Ferrate(1-) compound.
This synthetic route to Ferrate(1-) is commonly used in the chemical industry because it is relatively straightforward and can be carried out using readily available starting materials and reagents.
Additionally, the resulting compound has a number of important applications in various fields, such as pharmaceuticals, agrochemicals, and detergents, making it a valuable chemical for industrial applications.