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2-Bromo-9,9-di-n-butylfluoren is a synthetic compound that is commonly used in the chemical industry.
It is a colorless liquid with a characteristic smell, and it is soluble in organic solvents.
This compound is used as a building block in the synthesis of a variety of other chemicals, and it is also used as a solvent and in the production of various chemicals and materials.
One of the most common synthetic routes for 2-bromo-9,9-di-n-butylfluoren involves the reaction of 9,9-di-n-butylfluoren-2-ol with hydrogen bromide.
This reaction is typically carried out in the presence of a solvent, such as ether or benzene, and it is typically catalyzed by a strong acid, such as sulfuric acid or phosphoric acid.
The reaction is exothermic, and it is typically carried out at a temperature of between 80 and 100 degrees Celsius.
Another synthetic route for 2-bromo-9,9-di-n-butylfluoren involves the reaction of 9,9-di-n-butylfluoren-2-one with bromine in the presence of a solvent, such as carbon tetrachloride or chloroform.
This reaction is typically carried out at a temperature of between 60 and 80 degrees Celsius, and it is typically catalyzed by a Lewis acid, such as aluminum chloride or ferric chloride.
Yet another synthetic route for 2-bromo-9,9-di-n-butylfluoren involves the reaction of 9,9-di-n-butylfluoren with bromine in the presence of a solvent, such as acetone or methylene chloride.
This reaction is typically carried out at a temperature of between 20 and 30 degrees Celsius, and it is typically catalyzed by a Lewis acid, such as zinc bromide or ferric bromide.
Overall, there are several different synthetic routes for 2-bromo-9,9-di-n-butylfluoren, and the selection of a particular route will depend on a variety of factors, such as the cost and availability of the starting materials, the desired yield and purity of the product, and the reaction conditions.