The Production Process of Ethanesulfonic acid, 2-[[2-[[(3α,5β,7α,12α)-3,7,12-trihydroxy-24-oxocholan-24-yl]amino]acetyl]amino]-, sodium salt (1:1)

Ethanesulfonic acid, 2-[[2-[[(3α,5β,7α,12α)-3,7,12-trihydroxy-24-oxocholan-24-yl]amino]acetyl]amino]-, sodium salt (1:1) is a widely used intermediate chemical in the production of various pharmaceuticals, personal care products, and other industrial chemicals.
The production process of this compound involves several steps, including the synthesis of the starting materials, their purification, and the formation of the final product.

The synthesis of the starting materials involves the use of various chemical reactions and processes.
One of the key intermediate compounds used in the production of Ethanesulfonic acid, 2-[[2-[[(3α,5β,7α,12α)-3,7,12-trihydroxy-24-oxocholan-24-yl]amino]acetyl]amino]-, sodium salt (1:1) is 3,7-dihydroxy-24-oxocholan-24-amide.
This compound is synthesized by the reaction of 7-amino-3,3-bis(hydroxymethyl)-2,2-dimethylpropyl amide with 24-aminomethyl-24-hydroxycholan-3-amide in the presence of a base such as sodium hydroxide.
The reaction is carried out in a solvent such as dimethylformamide or dimethylacetamide and is followed by purification of the product using chromatography techniques.

Another key intermediate compound used in the production of Ethanesulfonic acid, 2-[[2-[[(3α,5β,7α,12α)-3,7,12-trihydroxy-24-oxocholan-24-yl]amino]acetyl]amino]-, sodium salt (1:1) is 3,7-dihydroxy-24-oxocholan-24-ylamine.
This compound is synthesized by the reaction of 24-hydroxycholan-3-amide with 7-amino-3,3-bis(hydroxymethyl)-2,2-dimethylpropylamine in the presence of a coupling agent such as dicyclohexylcarbodiimide in a solvent such as dimethylformamide.
The product is then purified using chromatography techniques.

Once the starting materials have been synthesized, they are purified to remove any impurities that may be present.
This is important to ensure the purity and consistency of the final product.
The purification process typically involves the use of chromatography techniques such as high-performance liquid chromatography (HPLC) or gas chromatography (GC).
These techniques involve the use of a stationary phase and a mobile phase to separate the compounds based on their chemical properties.

After the starting materials have been purified, they are combined and subjected to a series of chemical reactions to form the final product.
The specific reaction conditions and reagents used will depend on the starting materials and the desired product.
In the case of Ethanesulfonic acid, 2-[[2-[[(3α,5β,7α,12α)-3,7,12-trihydroxy-24-oxocholan-24-yl]amino]acetyl]amino]-, sodium salt (1:1), the reaction typically involves the use of a strong acid such as sulfuric acid to protonate the amide group of the starting material and form the final product.
The reaction is carried out in a solvent such as water or a polar organic solvent and is followed by purification using chromatography techniques.

Overall, the production process of Ethanesulfonic acid, 2-[[2-