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Diethyl-{2-[5-nitro-2-(4-propoxy-benzyl)-benzoimidazol-1-yl]-ethyl}-amine, also known as compound X, is a synthetic chemical compound commonly used in the field of organic chemistry.
It is a colorless liquid with a strong, unpleasant odor, and is soluble in many organic solvents.
The production process of diethyl-{2-[5-nitro-2-(4-propoxy-benzyl)-benzoimidazol-1-yl]-ethyl}-amine involves several stages, including synthesis, purification, and isolation.
The synthesis of compound X typically involves the use of specialized equipment and a variety of reagents and catalysts.
The first step in the production process is the synthesis of 5-nitro-2-(4-propoxy-benzyl)-benzoimidazole, also known as compound Y.
This compound is synthesized by reacting 4-propoxy-benzaldehyde with nitrosamine in the presence of a strong acid catalyst, such as hydrochloric acid.
The reaction is typically carried out at a temperature of around 80-90 degrees Celsius, and is followed by filtration and evaporation to remove any excess reagents.
Next, the synthesized compound Y is treated with diethyl-amine in the presence of a solvent, such as ethanol.
This reaction is carried out at a temperature of around 60-70 degrees Celsius, and is followed by filtration and evaporation to remove any excess reagents.
Finally, the resulting compound is purified and isolated by a process known as crystallization.
This involves dissolving the compound in a suitable solvent, such as ethanol or water, and allowing it to crystallize out of solution.
The crystals are then collected by filtration and washed with water to remove any impurities.
The final product is then dried and ground into a fine powder for use in various applications.
The production process of diethyl-{2-[5-nitro-2-(4-propoxy-benzyl)-benzoimidazol-1-yl]-ethyl}-amine is a complex and multi-step process that requires the use of specialized equipment and a variety of reagents and catalysts.
It is important to follow all safety precautions and guidelines when handling these chemicals, as they can be hazardous if not properly handled.