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The 3(2H)-Pyridazinone, 6-methyl-, hydrobromide (1:1) compound is an important intermediate in the synthesis of various pharmaceuticals, agrochemicals, and other chemical products.
The production process for this compound involves several steps, including synthesis, purification, and isolation.
In this article, we will take a detailed look at the production process for this compound, including the equipment and reagents required, the reaction conditions, and the purification and isolation methods used.
Synthesis
The synthesis of 3(2H)-Pyridazinone, 6-methyl-, hydrobromide (1:1) involves several stages, including the synthesis of the starting materials, the reaction of the starting materials to form the intermediate compound, and the reaction of the intermediate compound with hydrogen bromide to form the final product.
The starting materials for the synthesis of 3(2H)-Pyridazinone, 6-methyl-, hydrobromide (1:1) are typically obtained from commercial sources, such as Masada, Tokyo Research Chemical, and MolPort.
The starting materials are then subjected to a series of chemical reactions using standard organic synthesis techniques to form the intermediate compound.
Reaction Conditions
The synthesis of 3(2H)-Pyridazinone, 6-methyl-, hydrobromide (1:1) typically requires the use of anhydrous solvents, such as acetonitrile, dichloromethane, or ether, and certain catalysts, such as pyridine or triethylamine.
The reaction is typically carried out at temperatures between 50 and 80 degrees Celsius and under an inert atmosphere, such as nitrogen or argon.
Purification and Isolation
After the synthesis of the intermediate compound is complete, the product is typically purified and isolated using a series of methods, such as crystallization, precipitation, and chromatography.
These methods are used to remove any impurities that may have been introduced during the synthesis process and to obtain a pure sample of the final product.
Equipment and Reagents
The production process for 3(2H)-Pyridazinone, 6-methyl-, hydrobromide (1:1) requires the use of several pieces of equipment, including reaction vessels, rotary evaporators, and crystallization tanks.
In addition, a variety of reagents and solvents are required, including hydrogen bromide, pyridine, acetonitrile, dichloromethane, and ether.
Conclusion
The production process for 3(2H)-Pyridazinone, 6-methyl-, hydrobromide (1:1) involves several steps, including synthesis, purification, and isolation.
The process requires the use of specialized equipment and reagents and must be carried out in a controlled environment to obtain a pure sample of the final product.
The compound is an important intermediate in the synthesis of various pharmaceuticals, agrochemicals, and other chemical products, and its production is essential for the development of new and innovative chemical products.