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The production process of 3-chloro-6-(piperidin-4-yloxy)-pyridazine hydrochloride, also known as 98+% C9H13Cl2N3O, MW: 250.
12, involves several steps that require careful attention to detail and the use of specialized equipment.
The following is a detailed overview of the production process for this chemical compound.
Step 1: Preparation of raw materials
The production of 3-chloro-6-(piperidin-4-yloxy)-pyridazine hydrochloride begins with the preparation of raw materials.
This involves the synthesis of several precursor chemicals, which are then purified and dried to remove any impurities.
The specific raw materials used in the production of this compound are pyridazine hydrochloride, 3-chloropiperidine, and hydrochloric acid.
Step 2: Synthesis of 3-chloro-6-(piperidin-4-yloxy)-pyridazine
The next step in the production process is the synthesis of 3-chloro-6-(piperidin-4-yloxy)-pyridazine.
This is typically achieved through a series of chemical reactions, such as esterification, amination, and hydrolysis, which are carried out in a specialized laboratory using equipment such as reaction vessels, stirrers, and temperature controllers.
The specific steps involved in the synthesis of this compound may vary depending on the manufacturing process used.
Step 3: Purification of 3-chloro-6-(piperidin-4-yloxy)-pyridazine
After the synthesis of 3-chloro-6-(piperidin-4-yloxy)-pyridazine, the resulting product must be purified to remove any impurities that may have been introduced during the synthesis process.
This is typically achieved through a series of chromatography techniques, such as flash chromatography or high-performance liquid chromatography (HPLC).
The purified product is then dried using specialized equipment, such as vacuum dryers or fluid bed dryers, to remove any moisture or other impurities.
Step 4: Synthesis of 3-chloro-6-(piperidin-4-yloxy)-pyridazine hydrochloride
The final step in the production process is the synthesis of 3-chloro-6-(piperidin-4-yloxy)-pyridazine hydrochloride.
This is typically achieved through a process known as salt formation, in which the purified 3-chloro-6-(piperidin-4-yloxy)-pyridazine is mixed with hydrochloric acid to form the final product.
The resulting product is then dried and ground to the desired particle size using specialized equipment such as mills or micronizers.
Quality control:
After the production process is complete, the 3-chloro-6-(piperidin-4-yloxy)-pyridazine hydrochloride is subjected to a series of quality control tests to ensure that it meets the required specifications for purity, potency, and other characteristics.
These tests may include chemical analysis, microbiological testing, and physical testing, depending on the intended use of the product.
Any product that fails to meet the required standards is rejected and the production process is restarted from the beginning.
Conclusion:
The production process of 3-chloro-6-(piperidin-4-yloxy)-pyridazine hydrochloride, also known as 98+% C9H13Cl2N3O, MW: 250.
12, involves several steps that require careful attention to detail and the use of specialized equipment.
The production process begins with the preparation of raw materials, followed by the synthesis of 3-