The Production Process of 3-Chloro-6-(piperidin-3-ylMethoxy)-pyridazine hydrochloride, 98+% C10H15Cl2N3O, MW: 264.15

In the chemical industry, the production process of a particular compound is a critical aspect that involves various steps, from the synthesis of the starting materials to the purification and isolation of the final product.
In this article, we will discuss the production process of 3-Chloro-6-(piperidin-3-ylMethoxy)-pyridazine hydrochloride, a compound with a molecular formula of C10H15Cl2N3O and a molecular weight of 264.
15.

Step 1: Synthesis of Starting Materials
The synthesis of 3-Chloro-6-(piperidin-3-ylMethoxy)-pyridazine hydrochloride starts with the synthesis of its starting materials, which are 3-Chloro-6-(piperidin-3-ylMethoxy)pyridazine and hydrochloric acid.

3-Chloro-6-(piperidin-3-ylMethoxy)pyridazine can be synthesized through a variety of methods, including the reaction of 3-chloro-pyridazine with 6-bromo-piperidine in the presence of a solvent such as DMF.
The reaction produces the desired compound after a suitable reaction time and purification process.

Hydrochloric acid is another starting material that can be synthesized through various methods, such as the reaction of sodium chloride with hydrogen chloride gas or the reaction of iron chloride with hydrogen chloride gas.

Step 2: Condensation of Starting Materials
The next step in the production process of 3-Chloro-6-(piperidin-3-ylMethoxy)-pyridazine hydrochloride is the condensation of the two starting materials, which is achieved through a reaction known as a condensation reaction.
This reaction is carried out in the presence of a solvent such as ethanol, and a catalyst such as sodium hydroxide, at a suitable reaction temperature and time.

The condensation reaction produces 3-Chloro-6-(piperidin-3-ylMethoxy)pyridazine hydrochloride, which is insoluble in water but soluble in organic solvents such as methanol and ethanol.

Step 3: Purification and Isolation of the Final Product
After the condensation reaction, the final product is separated from the reaction mixture through a purification process, which typically involves crystallization, precipitation, or chromatography.
This step is critical in obtaining a pure and high-quality product.

In the case of 3-Chloro-6-(piperidin-3-ylMethoxy)-pyridazine hydrochloride, the final product is typically precipitated from a solution using a suitable precipitating agent, such as sodium chloride or hydrochloric acid.
The precipitated product is then filtered, washed with water, and dried to produce the final product.

Step 4: Characterization of the Final Product
The final step in the production process of 3-Chloro-6-(piperidin-3-ylMethoxy)-pyridazine hydrochloride is the characterization of the final product.
This involves a variety of tests and analyses, such as melting point, physical properties, chemical properties, and spectroscopic analysis.

The melting point of 3-Chloro-6-(piperidin-3-ylMethoxy)-pyridazine hydrochloride is typically determined using a melting point apparatus, which measures the temperature at which the compound changes from a solid to a liquid state.
The physical properties of the final product, such as its solubility and density, are also determined.

The chemical properties of the final product are assessed through various tests, such as the determination of its pH value,