-
Categories
-
Pharmaceutical Intermediates
-
Active Pharmaceutical Ingredients
-
Food Additives
- Industrial Coatings
- Agrochemicals
- Dyes and Pigments
- Surfactant
- Flavors and Fragrances
- Chemical Reagents
- Catalyst and Auxiliary
- Natural Products
- Inorganic Chemistry
-
Organic Chemistry
-
Biochemical Engineering
- Analytical Chemistry
-
Cosmetic Ingredient
- Water Treatment Chemical
-
Pharmaceutical Intermediates
Promotion
ECHEMI Mall
Wholesale
Weekly Price
Exhibition
News
-
Trade Service
The production process of 3-Bromo-N-(phenylmethyl)benzenesulfonamide, also known as 3-Bromo-N-(phenylmethyl)benzene sulfonamide or Brom phenyl, is a complex and multi-step process that involves several different chemical reactions and purification steps.
The final product is a yellow or light brown solid that is often used as a catalyst or as a pharmaceutical intermediate.
The production process can be divided into several main steps:
- Preparation of the starting materials
The first step in the production process is the preparation of the starting materials.
This includes the synthesis of the phenylmethyl group, which is used in the reaction to form 3-Bromo-N-(phenylmethyl)benzenesulfonamide.
This can be synthesized by several methods, including the reaction of phenylmethyl chloride with sodium hydroxide, followed by the addition of sodium bicarbonate and methyl iodide. - Nitration of benzene
The second step is the nitration of benzene, which is used as the starting material for the production of 3-Bromo-N-(phenylmethyl)benzenesulfonamide.
This is typically carried out using a mixture of nitric acid and sulfuric acid, which is known as nitrated sulfuric acid.
The reaction involves the addition of the nitrated sulfuric acid to benzene, with the formation of 3-nitrobenzene as a byproduct. - Sulfonation of 3-nitrobenzene
The third step is the sulfonation of 3-nitrobenzene, which involves the addition of sulfuric acid to the 3-nitrobenzene to form 3-Bromo-N-(phenylmethyl)benzenesulfonamide.
This reaction can be carried out using a variety of different reaction conditions, including the use of heat, ultrasonic energy, and/or solvents. - Purification of the product
The final step in the production process is the purification of the product.
This involves the removal of any impurities or side products that may have formed during the reaction.
This can be done using a variety of different methods, including crystallization, chromatography, and distillation. - Characterization of the final product
After the purification process, the final product is characterized to ensure that it meets the desired specifications.
This can include the use of techniques such as spectroscopy, mass spectrometry, and/or chemical tests.
In conclusion, the production process of 3-Bromo-N-(phenylmethyl)benzenesulfonamide is a complex and multi-step process that involves several different chemical reactions and purification steps.
The final product is a yellow or light brown solid that is often used as a catalyst or as a pharmaceutical intermediate.
The process involves the preparation of the starting materials, nitration of benzene, sulfonation of 3-nitrobenzene, purification of the product, and characterization of the final product.
The production process can be carried out using various conditions, and the product can be used in various industries.