The Production Process of [3,4-diacetyloxy-5-(4-amino-2-oxo-1,3,5-triazin-1-yl)oxolan-2-yl]methyl acetate

The production process of [3,4-diacetyloxy-5-(4-amino-2-oxo-1,3,5-triazin-1-yl)oxolan-2-yl]methyl acetate, also known as Compound X, involves several steps, including the synthesis of the starting materials, the reaction of these materials to form the intermediate compound, and the final steps to produce the final product.

The synthesis of [3,4-diacetyloxy-5-(4-amino-2-oxo-1,3,5-triazin-1-yl)oxolan-2-yl]methyl acetate begins with the synthesis of two key starting materials: 3,4-diacetyloxy-5-methyl oxolan-2-one and 4-amino-2-oxo-1,3,5-triazin-1-ylamine.

The synthesis of 3,4-diacetyloxy-5-methyl oxolan-2-one involves the reaction of methyl acetate with anhydroerythritol in the presence of an acid catalyst, such as sulfuric acid.
The reaction produces methyl acetate, which undergoes a series of condensation reactions to form the desired oxolan-2-one.
The final product is then treated with hydrobromic acid to introduce the diacetyl group.

The synthesis of 4-amino-2-oxo-1,3,5-triazin-1-ylamine involves the nitration of aniline with nitric acid, followed by reduction of the nitro group using a reducing agent, such as hydrogen gas or a metal reduction agent.
The resulting compound is then treated with an amine, such as piperidine, to introduce the amino group.

Once the starting materials have been synthesized, the next step in the production process is the reaction of these materials to form the intermediate compound, [3,4-diacetyloxy-5-(4-amino-2-oxo-1,3,5-triazin-1-yl)oxolan-2-yl]methyl acetate.
This reaction can be carried out using various methods, such as in a solution or in the solid state, and typically involves the use of a strong acid catalyst, such as sulfuric acid.
The reaction results in the formation of the desired intermediate compound.

The final step in the production process is the isolation and purification of the final product, [3,4-diacetyloxy-5-(4-amino-2-oxo-1,3,5-triazin-1-yl)oxolan-2-yl]methyl acetate.
This step typically involves the use of chromatography, such as high-performance liquid chromatography (HPLC), to separate the desired product from any undesired impurities.
The purified product is then collected and dried, resulting in the final, pure form of the compound.

In conclusion, the production process of [3,4-diacetyloxy-5-(4-amino-2-oxo-1,3,5-triazin-1-yl)oxolan-2-yl]methyl acetate involves the synthesis of two key starting materials, the reaction of these materials to form the intermediate compound, and the final steps to produce the final product.
The process requires the use of specialized equipment, such as chromatography systems, and the skills of trained chemical technicians to ensure the production of a high-quality final product.