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2-Chloro-7-cyclopentyl-7H-pyrrolo[2,3-d]pyrimidine-6-carboxylic acid, also known as CPPC, is a synthetic chemical compound that is commonly used in the production of various pharmaceuticals, agrochemicals, and other industrial products.
The production process of CPPC involves multiple steps, including synthesis, purification, and formulation.
In this article, we will outline the production process of CPPC in detail, highlighting the key steps and challenges involved in the manufacturing process.
Step 1: Synthesis of 7H-pyrrolo[2,3-d]pyrimidine-2,7-dione
The synthesis of CPPC begins with the production of 7H-pyrrolo[2,3-d]pyrimidine-2,7-dione, which is a key intermediate in the manufacturing process.
This compound is synthesized by a multi-step reaction process that involves the condensation of several precursor molecules.
The reaction process is carried out in a well-ventilated laboratory under strict safety protocols, as the precursor molecules used in the reaction can be hazardous if mishandled.
Step 2: Chlorination of 7H-pyrrolo[2,3-d]pyrimidine-2,7-dione
Once the 7H-pyrrolo[2,3-d]pyrimidine-2,7-dione has been synthesized, it is subjected to chlorination, which involves the addition of chlorine atoms to the molecule.
This step is carried out using a variety of chlorinating agents, such as thionyl chloride or phosphorus trichloride, in the presence of a solvent, such as dichloromethane.
The reaction is carefully monitored to ensure that the appropriate amount of chlorine is added, as excess chlorine can lead to the formation of unwanted byproducts.
Step 3: Purification of 2-Chloro-7-cyclopentyl-7H-pyrrolo[2,3-d]pyrimidine-6-carboxylic acid
The resulting product of the chlorination reaction is a mixture of compounds, which must be purified before further processing.
This purification process involves several steps, such as filtration, crystallization, and recrystallization, which are designed to remove impurities and improve the purity of the final product.
Step 4: Formulation of CPPC
Once the purified product has been obtained, it is formulated into the final product, which is used in various applications.
The formulation process involves mixing the purified product with other ingredients, such as excipients, solvents, and preservatives, to produce a stable and effective form of the product.
Production Scale and Cost
CPPC is typically produced on a large scale in a commercial manufacturing facility using industrial-scale equipment.
The cost of production depends on several factors, including the cost of raw materials, energy, and labor, as well as the scale of production.
The cost of CPPC can vary widely depending on the specific manufacturing process and the purity of the final product.
Quality Control and Regulations
The production process of CPPC must meet strict quality control standards to ensure that the final product is safe and effective for its intended use.
Quality control measures may include chemical and physical tests, such as melting point analysis, chromatography, and spectroscopy, to verify the purity and identity of the product.
In addition, the production of CPPC is subject to regulation by various government agencies, such as the Food and Drug Administration (FDA) and the Environmental Protection Agency (EPA), which set standards for the safety and environmental impact of the product.
Conclusion
The production process of CPPC involves several steps, from the synthesis of 7H-pyrrolo[2,3-d]pyrimidine-2,7-dione to the formulation of the final product.
The process requires strict adherence to safety protocols and quality control measures to ensure the