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2-(4-Bromophenyl)-6-iodoimidazo(1,2-a)pyridine, also known as IBX, is a commonly used pharmaceutical intermediate and research chemical.
The production process of IBX involves several steps, including the synthesis of the starting materials, the reaction of these materials, and the purification and isolation of the final product.
The synthesis of the starting materials involves the reaction of 4-bromophenyl chloride and imidazole in the presence of a solvent, such as ethyl ether or dichloromethane, and a catalyst, such as sulfuric acid or pyridine.
This reaction results in the formation of 2-(4-bromophenyl)-6-iodoimidazo[1,2-c]pyridine, also known as IBX.
The next step in the production process is the reaction of IBX with sodium iodide in the presence of a solvent, such as water or ethanol, and a catalyst, such as hydrochloric acid or sodium hydroxide.
This reaction results in the formation of 2-(4-bromophenyl)-6-iodoimidazo[1,2-a]pyridine, also known as IBX.
After the reaction is complete, the product is purified and isolated through a series of techniques, such as crystallization, filtration, and chromatography.
These techniques are used to remove any impurities and to obtain a pure sample of IBX.
The purified IBX is then dried and packaged for shipment to customers or for use in further processing.
The final product is a white or off-white crystalline powder that is highly soluble in water and other organic solvents.
In conclusion, the production process of IBX involves several steps, including the synthesis of the starting materials, the reaction of these materials, and the purification and isolation of the final product.
This process utilizes various chemical reactions and purification techniques to yield a pure sample of IBX, which is highly sought after in the pharmaceutical and research industries.