The operation method of hydrothermal synthesis reactor will take you to understand

Hydrothermal synthesis reactor is a commonly used small reactor in chemical laboratories, which can be used for small doses of synthetic reactions; It can also use the strong acid or alkali in the tank and the high temperature and high pressure closed environment to achieve the purpose of rapid digestion of
poorly soluble substances.
Operation method ◆ Pour the reactants into the PTFE bushing or PPL bushing, and ensure that the feeding coefficient is less than 0.
8
.
◆ Make sure that the position of the gasket under the kettle body is correct (the bulge faces down), then put in the PTFE bushing or PPL bushing and the upper gasket, first tighten the kettle cover, and then use the screw to twist and tighten the kettle cover
.
◆ Place the hydrothermal synthesis reactor in the heater and raise the temperature to the required reaction temperature
according to the specified heating rate.
(Less than the specified operating temperature)
。 ◆ When it is confirmed that the intra-abdominal temperature is lower than the boiling point of the reactant solvent, the lid of the kettle can be opened for subsequent operations
.
When it is cooled down at the end of the reaction, it should also be operated in strict accordance with the specified cooling rate to facilitate the service life
of the reactor.
◆ After confirming that the temperature in the kettle is lower than the boiling point of the reactant solvent, first use the screw to twist and loosen the kettle cover, and then open
the kettle cover.
◆ The hydrothermal synthesis reactor should be cleaned in time after each use to avoid rust
.
The sealing place of the kettle body and kettle cover line should be cleaned with special attention and strictly prevented from being damaged by bumps and damage
.