Begonia fruit triterpenes

Extract source: This product is the fruit of the red thick shell CalophyI Lum inophyllum Linn of the vine yellow plant extracted by the triamcinolone, the total content of triamcinolone is 80%the main ingredient: The ingredients of the hazelnut acid Oleanolic acid, content: 20%(with ingredients) sea otter sacin Canophylic acidcork triamcinol Friedelin28-hydroxyhaithol Canophyolcontent: 60%.s characteristics) this product is a white to pale yellow powder, soluble in methanol, ethanol, ortinol"Identification" take this product with methanol to make 0.5% solution for test ingeTake the standard sea otter serotonin, cork triamcinolone, 28-hydroxyseaol, zioic acid plus methanol to make the composition content of 1mg/ml solution for controlTake the red thick shell standard control of the medicinal herbs 1.0g plus 80% methanol 50ml, reflux extraction 30 minutes, filter steaming dry, residue plus 2.5mol/L sulphate 3ml, 100 c hydrolysis 2 hours, cooling, plus saturated with water isbutol extract 3 times, extraction with ammonia to pH 6 to 7, dehydration, steaming dryResidues plus methanol 1 ml make it dissolved as a control fluidTake the above three liquid each 10 sl, respectively, point on the same silicone G board, a point two board(1) expanded in cyclohexane-chloroform-ethyl acetate-ice acetate (20:5:8:0.5) and sprayed 10% ethanol sulfate solution, thermal wind blowing, under sunlight and UV lamp 365nm(2) is expanded with chloroform-methanol-isopropanol (16:0.5:0.25) and sprayed with a 5% vanilla alphic sulfate solution, which is blown by the hot windthe above two plates, the corresponding position of the standard speckle appears the same color spots, compared to the standard medicinal spots, the corresponding rate of 60%" Dry weightlessness: No more than 3.0% (Appendix IX.G)Burning Residue: No more than 0.6% (Appendix IX.J) Heavy Metals: No more than 10ppm (Appendix IX E) "content determination) according to the thin layer chromatography scanning method (appendix VI B) to determine the thin layer conditions thin layer plate: silicone G plate expander: cyclhexane-acetone acetate (5:2:1) color rendering agent: 10% sulphuric acid ethanol solution Color rendering method: spray, heating to color clear scanning condition wavelength: ss s 530nm s 700nm sample determination: take the standard of fruit acid and aqueous ethanol to make 0.5mg/ml solution, as a control solution Take this product and aqueous ethanol to make a 3mg/ml solution for test inge Take the control fluid: 4 sl, 8 sl and test fluid: 2 sl, intersection on the same thin layer plate, unfolded, color rendering, fixed, scanned, calculated in absorbance integral value, and calculated the total triamcinolone content " function" antibacterial, diuretic, analgesic, sputum storage is cool, dry and light-proof