Lyonsal alkaloids
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Last Update: 2020-06-12
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Source: Internet
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Author: User
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Extraction source: This product is a biobase ingredient extracted from the seeds of the crucirose plant radish Raphanus sativus Lwith a total alkaloid content of 80%main ingredients mustard alkali Sinapine, content: 30%p style"text-align: center; " img alt" "Lyuzial" src"/uploads/allimg/1701/2-1F1101G154631.jpg""style" Height: 194px; ,",- sein raphaninSulffen Sulforphen white mustard sinalbincontent: 50%the product is a light yellow to tawny powder, irritating, soluble in methanol, ethanol, acetone"Identification" take this product with methanol to make 0.5% solution for test ingeTake the standard mustard base, lysin, sulffen and other methanol to make each ingredient content of 1 mg / ml solution for controlTake the standard control of the medicinal herbs 1.0g plus ether 20 ml, ultrasonic degreasing for 20 minutes, discard ether solution, blow-dry residueAdd methanol to the residue 30 ml, ultrasonic extraction for 30 minutes, the filter concentrates to 1 ml of control fluidTake the above three liquid s5, respectively, point on the same silicone G board, to ethyl acetate-acetate-water (10:2:3) upper layer, ULTRAviolet lamp 365nm under the inspection, and then spray 1% vanilla aldehyde 10% sulfuric ethanol solution, hot wind showThe corresponding position of the standard speckle appears the same color fluorescent spots and visible spots, compared to the standard medicinal spots, the corresponding rate of 60%Dry weightlessness: No more than 3.0% (Appendix IX.G)Burning Residue: No more than 0.5% (Appendix IXJ)heavy metals: no more than 10ppm (Appendix IX.E) (content determination) according to high-efficiency liquid chromatography (appendix VI D) to determine the chromatography conditions benzene silane bonded silicone column flow phase: acetylene-3% ice acetic acid (15:85) detection wavelength: 326nm the ory plate number of 5000 the test solution: take this product with methanol to make a 120 sg/ml solution backup the determination: Take the above two liquid 5 sl injection liquid chromatography, and calculate the total alkaloid content the function of anti-pathogenic microorganisms, detoxification, cough, sputum, flat wheezing, improve urination function, lower blood pressure, anti-androgens storage is cool, dry and light-proof
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