Ibemaalalaline
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Last Update: 2020-06-12
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Source: Internet
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Author: User
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Extractsource: This product is the biobase composition extracted from the bulbs of Lily plants Xinjiang beema, Yili beema frit i Llaria pallidiflora Schrenk, with a total alkaloid content of 80%main ingredient: sibemino imperialine, content: 50%p style"text-style"text-center; "Img alt" "Ibemaalitine" src"/uploads/allimg/1702/2-1F202104AMN.jpg"style"style"width"width"width"" Height: 245px;.: Neobeninbase A, Sinbenebase B, Sinpeinine A, Sinpeinine B, Sinpeinine C Bemaisine Perisine Prirative sand meditone delavinonecontent: 30% -identification" take the product with chlorine imitation into 0.5% solution for test ingeTake the standard pinsibamine, bemalycin, neo-Benin base A, neo-Benin base B, neo-Benin base C and chlorine imitation into each containing 0.5 mg/ml solution for control solutionTake Ibe mother standard control of 1.0g ammonia water 1 ml, moist for 30 minutes, 30 ml of chloroform, 30 minutes ultrasonic extraction, the filter concentratetod to 1 ml for controlTake the above three liquid s6 sl, respectively, on the same silicone G-2% NaOH3 solution made of thin layer plate, with chloroform-ethyl ethyl-methanol-water (8:8:3:2) under the surface, first spray diluted potassium iodide test liquid, blow-dry, and then spray sodium nitrite test liquidThe corresponding position of the standard speckle appears the same color spot, compared to the standard medicinal spot, the corresponding rate of 60%" Dry weightlessness: No more than 2.0% (Appendix IX.G)Burning Residue: No more than 0.2% (Appendix IX.J)Heavy Metals: No more than 10ppm (Appendix IX.E)"Content Measurement" according to high-efficiency liquid chromatography (Appendix VI.D) determinationchromatography condition C18 columnmobile phase: acetylene-water-diathyamine (55:45:0.03)evaporative light scattering detector detection the number of theory boards is 3000 control fluid: take sibeimabase label with methanol to make 0.2 mg/ml solution backup test fluid: Take this product with methanol to make 0.4mg/ml solution backup the determination: take the above two-liquid 20 sl injection liquid chromatography, and calculate the total alkaloid content function to stop coughing, sputum, flat wheezing, decompression, lower blood pressure storage is cool, dry and light-proof
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