Fushou grass strong heart sideside

Extraction source: This product is a strong heartside ingredient extracted from the whole grass of adoms amurensis Reg.et Radde on the side of the wool, with a total strong heartside content of 80%(Main Ingredients) Bellan venomcose convallatoxin, content: 30%p style"text-align: center; " img alt" "Fushou grass heart side" src"/uploads/allimg/1612/2-1611131HFS41.jpg" Height: 230px;.." ., Canadian hempcym Cymarin toxic hair-haired cycloside K Strophanthoside KSomarin Somalincontent: 50%.s" this product is a white-to-pale yellow powder, soluble in methanol, ethanol"Identification" take this product with methanol to make 0.5% solution for test ingeTake the standard bell orchid venom, toxic hair spinoside, somarin and other methanol to make each ingredient content of 1 mg / ml solution for controlTake Fushou grass standard control of 1.0g with methanol 30 ml, ultrasound extraction for 20 minutes, the filter concentratetod to 1 ml of control fluidTake the above three liquid each 10 sl, respectively, point on the same silicone G board, a point two board(1) expanded with chloroform-dioxyx6-positive butol (70:20;5), spraying 20%3,5-dinitrophenylmethamphetamine ethanol solution, heating for 120 degrees C for 10 minutes, and then spraying 5% sodium hydroxide methanol solution(2) is expanded with ether, sprayed with 10% ethanol sulfate solution, hot wind blowingthe above two plates, the corresponding position of the standard speckle appears the same color spots, compared to the standard medicinal spots, the corresponding rate of 60%" Dry weightlessness: No more than 4.0% (Appendix IX.G)Burning Residue: No more than 0.8% (Appendix IX.J)Heavy Metals: No more than 10ppm (Appendix IX E) " content determination) according to the high-efficiency liquid chromatography (appendix VI D) to determine chromatography conditionS C18 column flow phase: methanol-water (65:35) flow rate: 0.8 ml / minute detection wavelength: 218nm standard curve: Take the bell-blue venomee standard with flow phase to make 1mg/ml solution, then add the flow phase dilution to the following concentrations: 20 sg/ml, 40 sg/ml, 60 sg/ml, 80 sg/ml, 100 ?l/ml, 120 sg/ml, 140?g/ml, 160?g/ml, 180?g/ml, 200?g/ml Each intake is measured by 5 sl, with the peak area sitting vertically, and the sample quantity (sg) as the horizontal coordinates, to be pictured sample determination: take this product plus flow phase to make 0.2mg/ml solution, sample 5 sl assay, and calculate the total strong heartside content function: strong heart, calm, hypnosis, live blood, detoxification, diuretic, anti-swelling storage is cool, dry and light-proof