Fine sin volatile oil

Extracted Source: This product is Horsebell Branch Fine Sin Asarum Sieboldii Miq., North Fine Sin Asarum Heterotropoides FrSchmidt.Mandshuricum (Maxim.) The volatile oil sizzle extracted from the weeds of Kitag., Seoul Fine Sin Asarum Sieboldii Miq.var.Seoulense Nakai, with a total volatile oil content of up to 80%

"main ingredient" methyl cloves phenolmethyleugenol, content: 30%

ssaric in

safrole

alpha-sanene alpha-rPinene

eu gyda'r cyhoeddus eu carvone

estrino estragole

thin brain Asarone

kadol Kakuol

content: 50%

"Character" this product is pale yellow to orange red clear, transparent liquid, can be mixed in petroleum ether, ether, chloroform, ethyl acetate

"Identification" take this product plus ether to make 0.5% solution for test solutionTake the standard products of methyl lilac phenol, fine ether, fine brain, jaundice and other ether to make each containing 4 mg / ml solution for control solutionTake fine xin standard control medicine 1.0g plus ether 30 ml, ultrasonic extraction for 30 minutes, steamed, residue plus ether 1 ml dissolved as a control liquidTake the above three liquids each 5 sl, respectively, point in the same silicone G board, with petroleum ether-ethyl acetate (9:1) to expand, spray 5% vanilla aldehyde sulfuric acid solution, hot wind blowingThe corresponding location of the label spot shows the same color spot, compared to the standard medicinal spot, the corresponding rate is 60%

"Check" fat oil: take this product 1g plus ethanol 10ml, shake well placed, no oil drips out

heavy metals: must not exceed 10 ppm (Appendix IXE)

"Content Determination" photogastography-mass spectrometry usage (appendix VI.E) assays

chromatography condition stoliano column: quartz capillary column, 0.32mm x 30m

column temperature: 40 to 120 degrees C

heating speed: 4 degrees C/min

gasification chamber temperature: 240 degrees C

gas: He

column front pressure: 68.6kPa

ionization: EI

ion source temperature: 200 degrees C

acceleration voltage: 4kV

control solution: take methyl clove phenol label plus waterless ether to make 2 ?g/ml, 3 sg/ml, 4 ?g/ml, 5 ?g/ml, 6 ?g/ml, 7 ?g/ml, 8 ?g/ml, 15 ?g/ml solution, with 10?l/ml of positive x-quadruple ether, each in the same as 0 l

sample determination: take this product 40 sl, n-than1l 10 sl, plus no water ether fixed capacity of 1 ml, take 0.13 sl sample determination

Volatile Oil Determination is measured by volatile oil determination (appendix XD)

antibacterial, anti-inflammatory, antiviral, anti-heat, numbness, analgesia, sedation, anti-alarm, blood pressure reduction, increase coronary artery blood flow, excited breathing

"storage" closed, cool, dry