Yellow Lian alkaloid

Extracted source: This product is the root extraction of biobase ingredients from the hairy plant huanglian Coptis chin: ensis Franch., triangular jaundice co-coptis deltoidea C.YCheng et Hsiao, cloud-linked Coptis teeta Wall., with a total biobase content of 80%main ingredients: small-alkali Berberine, content of 60%p style"text-style"text-center; " align " yellow alt" src"/uploads/allimg/1701/2-1F1051R104195.style"style: "style: 281px"; Height: 187px;Hot water"Identification" take this product with methanol to make 0.3% solution for test ingeTake the standard product small pyridine, table small pyridine, jaundice, methyl-yellow lycol and other methanol to make the content of each ingredient is 0.5 mg / ml solution for controlTake yellow link standard control medicine 0.5g with methanol 30 ml, ultrasonic extraction for 20 minutes, the filter concentrates to 1 ml for controlTake the above three liquids each 2 sl, respectively, point on the same silicone G board, to cyclhexhexyl-ethyl-ipropyl alcohol-water-triethylamine (3:3.5:1:1:1:0 5:1) unfolded, expanded before ammonia saturation, after the show blow-dry, under the UV lamp 365nm inspection, the corresponding position of the label spots show the same color fluorescent, the corresponding speckle specks of the same color, the corresponding species of the same speckle speckDry weightlessness: No more than 3.0% (Appendix IX.G)Burning Residue: No more than 0.5% (Appendix IX.J)Heavy Metals: No more than 10ppm (Appendix IXE) " content determination) according to the high-efficiency liquid chromatography method (appendix VID) to determinechromatography condition S18 columnmobile phase: acetylene 0.05mol/L phosphate dihydropotassium solution (50:50) (plus twelve alkyl per 100ml Sodium sulfate 0.4g, and then with phosphoric acid pH 4.0) detection wavelength: 345nm the number of theoretical plates s 5000 control liquid: take hydrochloric acid small pyridine standard with methanol to make 90.5 sg/ml solution backup for test fluid: take this product with methanol to make a 180 sg/ml solution backup the determination: take the above two liquid 10 sl injection liquid chromatography, and calculate the total alkaloid content : Anti-pathogenic microorganisms, anti-inflammatory, anti-diarrhea, vomiting, detoxification, elevated white blood cells, anti-cancer, deheating, analgesic, bile, sedation, enhanced immunity, excitable uterus, relaxation smooth muscle, blood pressure, blood lipids, blood sugar reduction, anti-cerebral ischemia, anti-arrhythmia, anti-cardiomyopathy, anti-platelet aggregation, anti-diabetic complications storage is cool, dry and light-proof