Yanhuso alkaloids

Extractsource: This product is a biobase extracted from tubers of the Yanhuso , Coyda Lis yanhusuo W.TWang, with a total alkaloid content of 80%main ingredients: Yanhuso ethyl Tetrahydropalma, content: 50%p style"text-align: center; " " " " " " " " " " " " " " " " " Yanhuso al-alkali" src" / uploads / allimg / 1702/2-1F201193495UHeight: 186px; .co.uk Corydaline original opioid base Protopinetetrahydro jaundice tetrahydrocoptisineYanhusin Corydalis Hsea poppy base Glaucine-bama Palmatinecontent: 30%Bitter, soluble in chloroform, ether, acetone, ethanolidentification" take the product with chlorine imitation into 0.5% solution for test ingeTake the standard pinahusso, yanhuso eth, yamussopropylene, ynhussodin, yamussosin, yanhusin, yanhusin with chlorine imitation into each containing 0.5mg/ml solution as a control solutionTake the standard control of 1.0g ammonia water 1 ml, moist for 30 minutes, with ether 40 ml, ultrasound extraction for 30 minutes, the filter steamed dry, residue plus chloroform 1 ml dissolved as a control liquidTake the above three liquid each 5 sl, respectively, on the same silicone G board, a point two board(1) to toluene-acetone (9:2), iodine vapor color, sunlight, and then waved iodine traces, UV lamp 365nminspection(2) to ether-cyclhexane-methanol (5:3:0.5), iodine vapor smoked for 1 minute, waved iodine, UV lamp 254nm inspection, and then the thin layer plate ammonia vapor steamed for 10 minutes, waved ammonia, and then ether-cyclhexane-methanol (5:3:0.5) secondary inspection, UV lamp 254nm inspection Finally, the third expansion of phenylchloroethylene-methanol digethamine (7:2:1:0.3) was expanded, and the UV lamp 365nm The corresponding position of the standard speckle appears the same color fluorescent spots and visible spots, compared to the standard medicinal spots, the corresponding rate of 60% Dry weightlessness: No more than 2.0% (Appendix IX.G) burning residue: No more than 0.1% (Appendix IX.J) Heavy Metals: No more than 10ppm (Appendix IX.E) "Content Determination" as high-efficiency liquid chromatography (Appendix VI.D) measurement chromatography condition C18 column mobile phase: methanol-0.1 phosphoric acid (triethylamine-modulation pH-6.0) (55:45) detection wavelength: 280nm the number of theory boards is 3000 control fluid: take the jen huso ethyl standard with methanol to make a 46 sg/ml solution backup the test solution: take this product with methanol to make a 92 sg/ml solution backup the determination: take the above-mentioned two-liquid 10 sl injection liquid chromatography, and calculate the total alkaloid content : Analgesia, sedation, hypnosis, stabilization, anti-allergy, inhibitgastric secretion, liver preservation, promote bile secretion, lower blood pressure, lower blood lipids, anticoagulant, antithrombotic ischemic hypoxia, dilated coronary arteries, excited pituitary adrenal system for Alzheimer's disease, arrhythmia storage is cool, dry and light-proof