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6-Chloro-N-ethylpyridazin-3-amine is a chemical compound that has a wide range of applications in the pharmaceutical, agricultural, and other industries.
It is a synthetic compound that is typically produced through a series of chemical reactions involving several intermediate products.
The synthetic routes of 6-chloro-N-ethylpyridazin-3-amine can vary depending on the starting materials and the desired product specifications.
One of the most common synthetic routes to produce 6-chloro-N-ethylpyridazin-3-amine involves a multi-step process that involves several chemical reactions.
The process typically starts with the reaction of ethyl-3-nitroacrylate with sodium azide in the presence of a solvent such as acetonitrile.
This reaction generates the intermediate compound ethyl-3-nitrosocyanate, which is then treated with ammonia and a catalyst such as palladium on barium carbonate to form 3-nitrosopyridine-2-carboxylate.
The next step in the synthesis of 6-chloro-N-ethylpyridazin-3-amine involves the reaction of 3-nitrosopyridine-2-carboxylate with chloroacetyl chloride in the presence of a solvent such as dichloromethane.
This reaction leads to the formation of 6-chloro-N-ethylpyridazin-3-amine.
Another synthetic route to produce 6-chloro-N-ethylpyridazin-3-amine involves a similar multi-step process that involves the reaction of ethyl 3-cyanopyrrolide-2-carboxylate with chloroacetyl chloride in the presence of a solvent such as dichloromethane.
This reaction leads to the formation of 6-chloro-N-ethylpyridazin-3-amine.
The synthetic routes of 6-chloro-N-ethylpyridazin-3-amine involve several chemical reactions that require careful control of the reaction conditions to ensure the desired product is obtained.
The reaction conditions can include temperature, pressure, solvent, and the presence of catalysts, reagents, and other chemicals that affect the outcome of the reaction.
The synthetic routes of 6-chloro-N-ethylpyridazin-3-amine can also be affected by the starting materials and the desired product specifications.
The choice of starting materials and the reaction conditions can affect the yield, purity, and other properties of the final product.
The synthetic routes of 6-chloro-N-ethylpyridazin-3-amine are typically carried out in a batch or continuous process, depending on the scale of production and the desired product specifications.
In a batch process, the reaction is carried out in a series of discrete steps, while in a continuous process, the reaction is carried out in a continuous flow of reactants and products.
The synthetic routes of 6-chloro-N-ethylpyridazin-3-amine can also involve the use of various chromatographic techniques to purify and separate the product from the byproducts and impurities.
These techniques can include gel filtration, high-performance liquid chromatography (HPLC), and other methods.
In conclusion, the synthetic routes of 6-chloro-N-ethylpyridazin-3-amine involve a series of chemical reactions that require careful control of the reaction conditions to ensure the desired product is obtained.
The choice of starting materials and the reaction conditions can affect the yield, purity, and other properties of the final product.
The synthetic routes of 6-chloro-N-ethylpyridazin-3-amine can be carried out in a batch or continuous