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The production process of methyl 6-oxo-1,6-dihydropyridazine-3-carboxylate involves several steps, which are carried out in a chemical plant.
The process can be broken down into the following stages:
- Preparation of starting materials
The first step in the production process is the preparation of the starting materials required for the synthesis of methyl 6-oxo-1,6-dihydropyridazine-3-carboxylate.
This involves the mixing of raw materials, such as ammonia, methanol, and hydrochloric acid, in appropriate ratios. - Condensation reaction
The next step in the production process is the condensation reaction.
In this reaction, the starting materials are heated and passed through a condenser, which removes any excess water formed during the reaction.
The reaction produces a liquid mixture of compounds, which is then cooled and collected. - Purification of the reaction mixture
The liquid mixture produced in the condensation reaction is then purified to remove any impurities that may have been produced during the reaction.
This is typically done using a variety of techniques, such as filtration, crystallization, and chromatography. - Hydrolysis reaction
The purified liquid mixture is then subjected to a hydrolysis reaction, which involves the addition of water to the mixture.
This reaction produces a solid precipitate, which is then collected and dried. - Recrystallization
The solid precipitate produced in the hydrolysis reaction is then purified further by the process of recrystallization.
In this process, the solid is dissolved in a suitable solvent and then allowed to crystallize out again.
The resulting crystals are then collected and dried to remove any impurities. - Characterization of the final product
The final step in the production process is the characterization of the final product.
This involves the determination of the chemical properties of the product, such as its molecular structure and composition.
This is typically done using a variety of techniques, such as spectroscopy, spectrometry, and chromatography.
In conclusion, the production process of methyl 6-oxo-1,6-dihydropyridazine-3-carboxylate involves several steps, which are carried out in a chemical plant.
The process involves the preparation of starting materials, a condensation reaction, purification of the reaction mixture, a hydrolysis reaction, recrystallization, and characterization of the final product.
The production process requires careful control and monitoring to ensure that the final product meets the required quality standards.