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The production process of ethanaminium, 2-[2-(acetyloxy)-1-oxopropoxy]-N,N,N-trimethyl-, 1,5-naphthalenedisulfonate (2:1), also known as N,N-dimethylacetamide-N-[(2S)-2-(acetyloxy)-1-oxopoyl]-2-(1,5-naphthalenedisulfonamido)amide, is a complex chemical reaction that involves several steps and intermediates.
The final product is a colorless to pale yellow liquid with a characteristic odor, and it is used in various applications in the chemical industry.
The production process of ethanaminium involves several steps, which can be broadly classified into the following:
- Preparation of the starting materials: The production process of ethanaminium starts with the preparation of the starting materials, which include acetic anhydride, 1,5-naphthalene dicarboxaldehyde, triethylamine, and dichloromethane.
These starting materials are mixed and combined in appropriate ratios to form the reaction mixture. - The reaction: The reaction mixture is then subjected to various chemical reactions, including condensation reactions, substitution reactions, and oxidation reactions.
These reactions result in the formation of intermediate compounds, which are further processed to form the final product. - Purification and isolation: The final product is then purified and isolated from the reaction mixture using various techniques, such as filtration, crystallization, and distillation.
These techniques help to remove any impurities and improve the purity of the final product. - Characterization: The final product is then characterized through various analytical techniques, such as spectroscopy, chromatography, and mass spectrometry, to confirm its identity and purity.
Let's take a closer look at each of these steps in more detail.
- Preparation of the starting materials: The starting materials for the production of ethanaminium include acetic anhydride, 1,5-naphthalene dicarboxaldehyde, triethylamine, and dichloromethane.
Acetic anhydride is a colorless liquid with a characteristic smell, and it is used as a catalyst in the reaction.
1,5-naphthalene dicarboxaldehyde is an orange liquid that is used as a reactant in the reaction.
Triethylamine is a clear liquid with a characteristic odor, and it is used as a base in the reaction.
Dichloromethane is a colorless liquid that is used as a solvent in the reaction. - The reaction: The reaction involves several steps, including condensation reactions, substitution reactions, and oxidation reactions.
The reaction starts with the condensation of 1,5-naphthalene dicarboxaldehyde and acetic anhydride, which results in the formation of 1,5-naphthalene dicarboxylic acid.
This intermediate is then reacted with triethylamine to form the N-[(2S)-2-(acetyloxy)-1-oxopoyl]-2-(1,5-naphthalenedisulfonamide)amide intermediate.
The final product, ethanaminium, is then formed through an oxidation reaction that involves the addition of 1,5-naphthalene dicarboxaldehyde to the N-[(2S)-2-(acetyloxy)-1-oxopoyl]-2-(1,5-naphthalenedisulfonamide)amide intermediate. - Purification and isolation: The final product is then purified and isolated from the reaction mixture using various techniques, such as filtration, crystallization, and distillation.
These techniques help to remove any imp