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The Production Process of 4-Pyridinol,5-amino-2-chloro-(9CI) in the Chemical Industry
4-Pyridinol,5-amino-2-chloro-(9CI) is a widely used intermediate in the production of various chemicals and pharmaceuticals.
The chemical formula for this compound is C5H5ClN2O.
It is primarily used as a building block for the synthesis of other compounds and has various applications in the production of drugs, agrochemicals, and dyes.
The production of 4-Pyridinol,5-amino-2-chloro-(9CI) involves several steps, each of which must be carried out with great care and precision to ensure that the final product is of the highest quality.
In this article, we will take a closer look at the production process for this compound, including the various techniques and equipment used in each step.
Step 1: Raw Material Preparation
The production of 4-Pyridinol,5-amino-2-chloro-(9CI) begins with the preparation of raw materials.
The primary raw material used in the production of this compound is ammonia gas, which is converted into ammonium hydroxide through a series of chemical reactions.
The ammonium hydroxide is then used to synthesize 4-Pyridinol,5-amino-2-chloro-(9CI) through a series of chemical reactions.
Step 2: Oxy-Chlorination
The next step in the production process is oxy-chlorination.
In this step, chlorine gas is added to a mixture of water and sodium hydroxide.
The mixture is then heated, causing the chlorine gas to react with the water and sodium hydroxide to form a solution of sodium chlorate.
This solution is then used in the next step of the production process.
Step 3: Hydrolysis
The sodium chlorate solution from the previous step is then subjected to hydrolysis, which involves the addition of water to the solution.
This reaction causes the formation of sodium hydroxide and hydrogen chloride gas.
The hydrogen chloride gas is then used in the next step of the production process.
Step 4: Nitration
The next step in the production process is nitration, in which nitric acid is added to the hydrogen chloride gas from the previous step.
This reaction causes the formation of 4-chloro-5-nitro-2-pyridine.
The resulting compound is then used in the next step of the production process.
Step 5: Reduction
In the final step of the production process, the 4-chloro-5-nitro-2-pyridine compound is subjected to reduction.
This involves the addition of a reducing agent, such as hydrazine, to the compound.
The reaction causes the conversion of the compound into 4-Pyridinol,5-amino-2-chloro-(9CI), which is the final product.
Equipment Used in the Production Process
The production of 4-Pyridinol,5-amino-2-chloro-(9CI) requires the use of specialized equipment to ensure that the process is carried out safely and efficiently.
Some of the key equipment used in this production process include:
- Chlorination tanks: These tanks are used to add chlorine gas to the mixture of water and sodium hydroxide.
- Hydrolysis tanks: These tanks are used to add water to the sodium chlorate solution, causing the formation of sodium hydroxide and hydrogen chloride gas.
- Nitration