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Introduction
In the chemical industry, the production of various chemical compounds is a complex process that involves several stages.
The production of [1,1′-Biphenyl]-3-carboxylic acid, 3′-amino-, methyl ester is a critical step in the manufacture of several important chemical products.
This compound is commonly used in the production of insecticides, herbicides, and other agricultural chemicals.
In this article, we will discuss the production process of [1,1′-Biphenyl]-3-carboxylic acid, 3′-amino-, methyl ester.
Raw Materials
The production of [1,1′-Biphenyl]-3-carboxylic acid, 3′-amino-, methyl ester requires a variety of raw materials, including 1,1′-biphenyl, carboxylic acid, ammonia, and methanol.
These raw materials are first obtained from their respective sources, and then purified to remove any impurities that may interfere with the production process.
Preparation of the Starting Material
The preparation of the starting material involves the reaction of 1,1′-biphenyl with carboxylic acid in the presence of a catalyst.
This reaction produces the desired biphenyl ester, which is then treated with ammonia and methanol to form the final product.
The reaction is carried out under controlled conditions, such as temperature, pressure, and time, to ensure that the product is of the desired quality.
Chemical Reactions
The primary chemical reaction involved in the production of [1,1′-Biphenyl]-3-carboxylic acid, 3′-amino-, methyl ester is the reaction between 1,1′-biphenyl and carboxylic acid.
This reaction is catalyzed by a strong acid catalyst, such as sulfuric acid or phosphoric acid.
The reaction produces the desired biphenyl ester, which is then treated with ammonia and methanol to form the final product.
The chemical reaction can be represented by the following equation:
1,1′-Biphenyl + Carboxylic Acid → Biphenyl Ester
The biphenyl ester produced in this reaction is then treated with ammonia and methanol to form the final product.
The reaction is carried out under controlled conditions, such as temperature, pressure, and time, to ensure that the product is of the desired quality.
Ammonolysis
The ammonolysis reaction involves the treatment of the biphenyl ester with ammonia and methanol to form the final product.
This reaction is carried out in the presence of a strong acid catalyst, such as sulfuric acid or phosphoric acid.
The reaction produces the desired [1,1′-Biphenyl]-3-carboxylic acid, 3′-amino-, methyl ester, which is then purified to remove any impurities that may be present.
The chemical reaction can be represented by the following equation:
Biphenyl Ester + Ammonia + Methanol → [1,1′-Biphenyl]-3-carboxylic acid, 3′-amino-, methyl ester
Purification
After the production of [1,1′-Biphenyl]-3-carboxylic acid, 3′-amino-, methyl ester, the product is purified to remove any impurities that may be present.
This purification process involves the use of various techniques, such as distillation, crystallization, and chromatography.
The purified product is then packaged and stored for later use.
Conclusion
In conclusion, the production