Huashan ginseng alkaloid

Extract source: This product is a biobase ingredient extracted from the roots of eggplant funnel vesyllasPh Physochlainainfundiularis Kuang, with a total alkaloid content of 80%main ingredient: zirconic Hyoscyamine, content: 30%p style"text-align: center; " img alt" "Huashan ginseng alkaloid" src"/uploads/allimg/1612/1612GQ243I1.jpg" Height: 172px; " saary anisodamineScopolamineRed ancient beanbase Cuscohygrine Atropine atropinecontent: 50%.the product is a white-to-pale yellow powder, soluble in chloroform, ether, acetone, and ethanolidentification" take the product with chlorine imitation into 0.5% solution for test ingeTake the standard product of the alkali, hawthorn alkali, the eastern fentech, atropine chlorine imitation into the composition content of 1mg/ml solution as a control solutionTake Huashan ginseng standard control medicine 1.0g ammonia-based water ethanol (1:1) solution 2 ml wet, chlorine chloride 30 ml, reflux extraction for 40 minutes, filter steamed dry, residue plus chloroform 1 ml dissolved as a control liquidTake the above three liquids each 5 sl, respectively, point on the same silicone G board, to ethyl acetate-methanol ammonia water (17:2:1) to expand, first spray potassium iodide test liquid, inspection, and then spray sodium nitrite ethanol test liquid, the corresponding position of the label spots show the same color spots, compared to the standard medicinal spots, the corresponding rate of more than 60%" Dry weightlessness: no more than 3.0% (Appendix IX.G)burning residue: not more than 0.5% (Appendix IX.J)Heavy Metals: No more than 10ppm (Appendix IX.E)"Content Measurement" according to the high-efficiency liquid chromatography (Appendix VID) To determine thechromatography condition S18 columnflow phase: 1/15mol/L sodium phosphate solution (phosphate pH-3.5) - methanol (48:52) (containing 17.5mmol/L sodium diaxalsulfylate)column temperature: 35 degrees C detection wavelength: 210nmstandard curve internal label solution: 210nm amine-based methanol 0.2 mgthe use of pyridine and chlorine imitation into 1 mg/ml solution for storagetake 0.2 ml of storage fluid, plus 2 ml of internal label fluid, plus flow phase is compatible at 10 ml, for 20 sg/ml solutionIf the method is formulated 40 ?g/ml, 60 ?g/ml, 80 ?g/ml, 100 ?g/ml solution, each take 10 ?l injection liquid chromatography assays, to be plottedregression equation: Y-0.8005X-2.557 x (-1000)sample determination: take the product with chlorine to 3mg/ml solution, take 0.4 ml plus the standard liquid 2 ml, add flow phase to 10 ml, take 10 sl injection liquid chromatographic determination, and calculate the total biobase contentfunctions to improve microcirculation, anticoagulant, anti-cerebral ischemia, anti-reperfusion damage, anti-vibration fibrillation, analgesic, despasm relief, memory, speed up heart rate, dilated trachea, antioxidant, central inhibitionstorage is cool, dry and light-proof