How to use a double-glazed reactor

Double glass reactor is a kind of experimental equipment integrating vacuum, distillation, reflux, stirring, constant temperature water bath or oil bath, which can carry out various biochemical reactions and synthesis reactions
under constant temperature conditions.
The use of double-glazed reactor is as follows: (1) Check whether the power supply voltage is the same as the specifications provided on the
machine nameplate.
(2) Plug in the power plug, turn on the power switch on the inverter, and use the speed control knob to select the appropriate speed
.
(3) The flow of materials and the power of motor speed may resonate at a certain point, please change the speed of the motor to avoid resonance
.
(4) After the stirring rod is installed, it must be rotated by hand, pay attention to whether the concentricity is good, just as the centricity is not good, the heavy clamp should be released, and then turn on the power after clamping, and gradually adjust
from slow to fast.
(5) Using the stirring rod adjuster, the stirring leaves can be made up and down 5cm
as needed.
(6) If you find that the sealing performance of the kettle is reduced, please check the rotating bearing
in the agitator sleeve.
(7) Self-equipped reaction bottles and other glass instruments, please confirm the quasi-glass material to ensure safe use
.
(8) The interlayer on the glass kettle is connected to the external circulation port, through the hot oil can do heating reaction, can be on the coolant can carry out low temperature reaction, if the use of steam heating, should not exceed 0.
5K-1K
.
(Try not to use pressure steam heating)
。 (9) When testing at low temperatures, the bottom discharge valve will frost, and the valve must be thawed locally first to prevent the glass
from being broken.
(10) If there are particulate objects in the solution in use, there may be accumulation of residues on the PTFE piston of the valve when discharging, and the air tightness will be affected when used again, so be sure to clean and use
again after each discharge.