Helippi seroine
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Last Update: 2020-06-12
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Source: Internet
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Author: User
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Extract source: This product is a triamcine saponin ingredient extracted from the bark of the bean plant hemal Albizia jutibrissin Durazz(Main Ingredients) Echinocyctic acid, content: 20%p style"text-align: center; Height: 195px;.." ..) Hehdine AllibisideHealy-Julibroside Heyotriano-Julibroside Heibrotriterpenal lactoneMekiberic acid MachaerinicContent: 60%.s trait) This product is a pale yellow to yellow brown powder, soluble in methanol, thin ethanol, and water-containing"Identification" take this product with methanol to make 0.5% solution for test ingeTake the standard stingant cystic acid, helicoside, helicoside and other methanol to make each component content of 1 mg / ml solution for controltake of the skin standard control of 1.0g plus 50% methanol 30 ml, ultrasonic extraction 30 minutes, the filter steamed dry, residue plus methanol 1 ml to dissolve as a control liquidTake the above three liquids each 5 sl, respectively, point on the same silicone G board, to chloroform-methanol-water (13:5:2) lower layer expansion, spray 5% phosphorus argon ethanol solution, hot wind blowing, the corresponding position of the standard spot appears the same color spots, compared to the standard medicinal spots, the corresponding rate of 60%" Dry weightlessness: No more than 3.0% (Appendix IX.G)Burning Residue: No more than 0.5% (Appendix IXJ)Heavy metals: no more than 10ppm (Appendix IX.E)(content determination) according to the high-efficiency liquid chromatography (appendix VI.D) to determinechromatography conditions C18 columnflow phase: methanol-water (80:20)column temperature: 40 oCdetection wavelength: 215 nmstandard curve to pick up cystic acid standard 23.4 mg dissolved in 25 mlThe storage liquid is 0.4 ml, 2 ml, 4 ml, 6 ml, 8 ml, 10 ml, respectively, with methanol fixed at 10 ml, each taking 20 sl, injected with a liquid chromatograph, to peak area ordinate, concentration for horizontal coordinates, for mappingregression equation : Y 4.436 x l00000000 x 7.158 x 1000000 linear range: 0.18 to 0.90mg/mlsample determination: take this product plus methanol into 1.5mg/ml solution, take 20 l injection liquid chromatograph, and calculate the total acid contentfunction: sedation, hypnosis, enhanced immunity, resistance to pathogenic microorganisms, insect repellent, anti-cancer, anti-fertility, anti-coagulationstorage is cool, dry and light-proof
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