Hainan dog tooth flower alkaloid

Extraction source: This product is the root extraction of the root of the hainan dog tooth flower Ervatamia Hainannsis Tsiang, the total alkaloid content of 80%(Main Ingredients) Dog Tooth Flower Alkaline Coronaridine, content: 40%"text-style"text-type": center; "align" "Hainan dog tooth flower alkaloid" src"/uploads/allimg/1701/2-1F1051I3020.jpg"style" Height: 151px; :: HeyneanineOld hedgehog base Vobasine Porifine base PerixmeIbominbase Ibogaminecontent: 40%.the character is a white to pale yellow powder, soluble in chloroform, ether, ethyl acetate, acetone, ethanolidentification" take the product with chlorine imitation into 0.5% solution for test ingeTake the standard dog tooth base, haeinine base, old hedgehog base and other chlorine imitation into the content of each ingredient is 1mg/ml solution for controlTake Hainan dog tooth flower standard control medicine 1.0g ammonia water 0.5 ml, moist for 30 minutes, 30 ml of chloroform, heating reflux extraction for 30 minutes, the filter concentrates to 1 ml for controlTake the above three liquid each 5 sl, respectively, on the same silicone G board, a point two board(1) is carried out in chloroform-methanol (8:2) and sprayed with potassium iodide(2) to ethyl acetate-methanol-ammonia (17:2:1) to spray improved potassium iodide test fluidthe above two plates, the corresponding position of the standard speckle appears the same color spots, compared to the standard medicinal spots, the corresponding rate of 60%" Dry weightlessness: No more than 3.0% (Appendix IX.G)Burning Residue: No more than 0.6% (Appendix IX.J)Heavy Metals: No more than 10ppm (Appendix IXE)content determination) according to the thin layer chromatography (appendix VIB) to determine thethin layer conditions thin layer plate: silicone GF254 plate, 105 degrees C activated 60 minutesexpander: chloroform-methanol-petroleum ether (9:1:5)scanning condition scanning wavelength: ss s280nms Two-wavelength thin-layer scanningscattering parameters: SX-3 Standard curve Take dog's cofactory base standard with methanol to make a 1mg/ml solution, take 2 sl, 4 sl, 6 sl, 8 sl, 10 sl points in the same thin sheet, expand, scan, with peak area coordinates, with a pattern amount (sg) as horizontal coordinates, as plottedsample assay: take this product with methanol to make 2mg/ml solution, take 2 sl intersection in the control liquid: 2 ?l, 4 ?l in the same plate, unfold, blow-dry, fix, scan, calculate, and calculate the total alkaloid contentfunction: lower blood pressure, lower blood lipids, anti-atherosclerosis, heat, detoxification, swelling, analgesia, estrogen-like effectstorage is cool, dry and light-proof