Flying Dragon Palm Blood Alkaloid

Extractsource: This product is the root extraction of alkaloid strains of the fennel plant the moth palm blood Todda Asiatica Lam(main ingredients) White-chostisse red-alkali Chelerythrine, content: 50%p style"text-align: "text-align": center;" src"/uploads/allimg/1612/2-1612133Q996.jpg" Height: 155px; .dihydro-white-chocho-erythrineskimyanine the skimyaninefeline palm blood mothebase Toddalidimerine thecontent: 30%the "sex" is a red-yellow to brownpowder powder, soluble in chloroform, ether, ether, ether, and etheroniteidentification" take the product with chlorine imitation into 0.5% solution for test ingeTake the standard white leek red alkali, taro alkali, flying dragon palm blood molybdenum and other chlorine imitation into the content of each ingredient is 1mg /ml solution forcontrol liquidTake the moth palm blood standard control medicine 1.0g ammonia water 0.2 ml after 2 hours, 40 ml of chloroform, reflux extraction for 30 minutes, the filter concentrated to 1 ml for controlTake the above three liquid each 10 sl, respectively, point on the same silicone G board, a point two board(1) is expanded with positive butyl alcohol iced acetic acid (95:5)(2) is expanded with chloroform-methanol (9:1)spray edion potassium iodized potassium test liquid, the corresponding position of the standard speckle appears the same color spot, compared to the standard medicinal species, the corresponding rate of 80%Dry weightlessness: No more than 4.0% (Appendix IX.G)Burning Residue: No more than 0.8% (Appendix IX.J) Heavy Metals: No more than 10ppm (Appendix IX E) "content determination" according to the high-efficiency liquid chromatography (appendix VI D) to determine the chromatography condition S18 pillar mobile phase: acetylene-0.1% sulfuric acid (25:75) detection wavelength: 270nm standard curve to take white leek red alkale plus Methanol is made into 0.1mg/ml for control storage fluid, with a control reserve fluid plus methanol, diluted to 2 ?g/ml, 4 ?g/ml, 10 ?g/ml, 12 ?g/ml, 16 ?g/ml, each with 5 sl injection liquid chromatographic assays, with peak area ordinates, to sample (ng) as horizontal coordinates, pictured Regression equation: Y-18022864X-2916.8072 linear range: 1 to 72 ng sample determination: take this product with methanol to make a solution of 4 ?g/ml, take 10 sl injection liquid chromatography, and calculate the total biopic content function anti-inflammatory, analgesic storage is cool, dry and light-proof