Customs vine saponins

Extract source: This product is For The Ramoco Plant Pass Vine Marsdenia Tenacissima (Roxb.) Wight et Am.'s vine extracted saponin sourin serombine composition with a total saponin content of 80%(Main Ingredients) Customs K Tenacissoside K, content: 30%p style"" text-align: center; Height: 217px; "Img alt""""src"/uploads/allimg/1701/2-1F1231G034938.jpg" style": "width: 503px; height: 346px; ""'s ingredients" (ingredients) Marsdekoisidecontent: 50%"character" this product is milky white to light brown powder, soluble in methanol, lean ethanol, water-containing positive butanol"Identification" take this product with methanol to make 0.5% solution for test ingeTake the standard product customs pass vinegshh H, customs rattan glycoside J, customs vine glycoside K, milk vegetable glycoside plus methanol to make each containing 1mg/ml solution for controlTake the standard control of the rattan 1.0g water-saturated positive butanol 30 ml, ultrasonic extraction for 30 minutes, the filter concentrated to 1 ml of control liquidTake the above three liquids each 6 sl, respectively, point on the same silicone G board, to chloroform-acetone-methanol (18:10:6) to expand, spray vanilla aldehyde sulfuric acid test liquid, hot wind showThe corresponding position of the standard speckle appears the same color spot, compared to the standard medicinal spot, the corresponding rate of 60%" Dry weightlessness: No more than 3.0% (Appendix IX.G)burning residue: No more than 0.5% (Appendix IX.J)Heavy Metals: No more than 10ppm (Appendix IX.E)"Content Measurement" according to thin layer chromatography (Appendix VI.B) determinationthin layer conditions: thin layer board: silicone G boardexpander: chloroform-acetone-methanol (15:10:5)color rendering agent: vanilla aldehyde sulfuric acid test liquid color rendering method: After spraying, bake to the spot clarity at 105 degrees C scan condition wavelength: ss s.325nm r-R-600nm scan: Reflected jagged scan slit: 1.25rnm x 1.25mm scattering parameter: SX.3 the standard curve to take the customs vine glycoside K standard with methanol to make 1.2mg/ml solution It is divided into 1 ?l, 5 ?l, 10 ?l, 15 ?l, 20 ?l, 25 ?l, and 30 ?l, respectively, at the same thin layer plate, expanded, scanned Map the peak area in a dot- amount sample assay: Take this product with methanol to make a 4.0mg/ml solution The intersection points of 5 ?l and 10 ?l are taken in 5 ?l, 10 ?l, and the control fluid: 1 ?l, 5 ?l, and 10 ?l intersection sit at the same thin plate, expanded, scanned The content is calculated by the standard curve and the total saponin content is calculated " function" antibacterial, anti-inflammatory, cough, sputum, flat wheezing, milk storage is cool, dry and light-proof